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The Manhattan Project Heritage Preservation Association, Inc. "Preserving, Exhibiting, Interpreting and Teaching the History of the Manhattan Project" |
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Manhattan Project History
Manhattan Engineer District
Isotope Separation & Plutonium - Fall 1942
| "Perhaps today was the most exciting and thrilling day I have experienced. Our microchemists isolated pure element 94 (plutonium) for the first time...It is the first time that element 94 has been beheld by the eye of man." - Glenn Seaborg; Metallurgical Laboratory; University of Chicago; August 20, 1942 |
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Groves made good on his timetable when he scheduled a meeting of the Military Policy Committee on November 12 and a meeting of the S-1 Executive Committee on November 14. The scientists at each of the institutions doing isotope separation research knew these meetings would determine the separation method to be used in the bomb project; therefore, the keen competition among the institutions added to the sense of urgency created by the war. Berkeley remained a hotbed of activity as Lawrence and his staff pushed the electromagnetic method into the lead. The S-1 Executive Committee even toyed with the idea of placing all its money on Lawrence but was dissuaded by Conant. Throughout the summer and fall, Lawrence refined his new 184-inch magnet and huge cyclotron to produce "calutrons", as the tanks were called in honor of the University of California, capable of reliable beam resolution and containing improved collectors for trapping the enriched uranium 235. The S-1 Executive Committee visited Berkeley on September 13 and subsequently recommended building both a pilot plant and a large section of a full-scale plant in Tennessee. The centrifuge being developed by Jesse Beams at the University of Virginia was the big loser in the November meetings. Westinghouse had been unable to overcome problems with its model centrifuge. Parts failed with discouraging regularity due to severe vibrations during trial runs; consequently, a pilot plant and subsequent production stages appeared impractical in the near future. Conant had already concluded that the centrifuge was likely to be dropped when he reported to Bush on October 26. The meetings on November 12 and 14 confirmed his analysis. Gaseous diffusion held some promise and remained a live option, although the Dunning group at Columbia had not yet produced any uranium 235 by the November meetings. The major problem continued to be the barrier; nickel was the leading candidate for barrier material, but there was serious doubt as to whether a reliable nickel barrier could be ready in sufficient quantity by the end of the war. While the centrifuge was cancelled and gaseous diffusion received mixed reviews, optimism prevailed among the pile proponents at the Metallurgical Laboratory in Chicago. Shortages of uranium and graphite delayed construction of the Stagg Field pile (CP-1; Chicago Pile Number One), but this frustration was tempered by calculations indicating that a completed pile would indeed produce a chain reaction. With Enrico Fermi's move to the Met Lab in April (from Columbia), all pile research was now being conducted at Chicago as Compton had planned, and Fermi and his team anticipated a successful experiment by the end of the year. Further optimism stemmed from Glenn Seaborg's inventive work with plutonium, particularly his investigation on plutonium's oxidation states that seemed to provide a way to chemically separate plutonium from the irradiated uranium to be produced in the pile. In August, Seaborg's team produced a microscopic sample of pure plutonium, a major chemical achievement and one fully justifying further work on the pile. The only dark cloud in the Chicago sky was the scientists' disappointment when they learned that construction and operation of the production facilities (including the semi-works), now to be built near the Clinch River in Tennessee at Site X, would be turned over to a private firm (du Pont). A second experimental pile (CP-2) would be built in the Argonne Forest Preserve just outside Chicago, but the Metallurgical Laboratory scientists would have to cede their claim to pile technology to an organization experienced enough to take the process into construction and operation.
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